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Revision 004, 12/09 v
© SP Industries, Inc. 2009
Contents
Important Symbols ............................................................................................................................................... ii
Freeze Dryer Safety Warnings............................................................................................................................. ii
Warranty Information .......................................................................................................................................... iii
Introduction............................................................................................................................................ 1
Key Features........................................................................................................................................................1
BenchTop Usage .................................................................................................................................................1
Available Configurations ......................................................................................................................................2
From Freeze Dryer to Condenser Module............................................................................................................2
Cold Trap Condenser Module ..............................................................................................................................2
Installation and Setup ........................................................................................................................... 3
Initial Inspection ...................................................................................................................................................3
Service Connections ............................................................................................................................................3
Vacuum Pump Installation ...................................................................................................................................4
Installing the Vacuum Pump............................................................................................................................4
Oil Mist Eliminators..........................................................................................................................................5
Freeze Dryer Setup..............................................................................................................................................6
Vacuum Baffle Plate ............................................................................................................................................7
Freeze-Drying Concepts ....................................................................................................................... 9
Elements of Freeze-Drying ..................................................................................................................................9
Freeze .............................................................................................................................................................9
Vacuum ...........................................................................................................................................................9
Heat...............................................................................................................................................................10
Condenser.....................................................................................................................................................10
Product Dependencies.......................................................................................................................................10
Sentry 2.0 Controls.............................................................................................................................. 11
LED Wave Display (Qualitative Reference) .......................................................................................................11
Button Functions ................................................................................................................................................12
Up/Down (+/-) Buttons...................................................................................................................................12
MENU Button ................................................................................................................................................12
COND Button ................................................................................................................................................12
VAC Button....................................................................................................................................................12
AUTO Button .................................................................................................................................................12
DEFR Button .................................................................................................................................................12
LCD Display Functions ......................................................................................................................................13
Main Menu .........................................................................................................................................................13
Vacuum Control.............................................................................................................................................14
Purge (Optional) ............................................................................................................................................14
Heat (Optional) ..............................................................................................................................................14
User Options Menu ............................................................................................................................................14
Vacuum Control.............................................................................................................................................14
Temperature Units.........................................................................................................................................15
Vacuum Units ................................................................................................................................................15
- VirTis BenchTop 2K, 4K and 6K 1
- Important Symbols 4
- Freeze Dryer Safety Warnings 4
- Warranty Information 5
- Contents 7
- Revision 004, 12/09 vii 9
- © SP Industries, Inc. 2009 9
- Introduction 11
- Available Configurations 12
- Cold Trap Condenser Module 12
- Installation and Setup 13
- Vacuum Pump Installation 14
- Oil Mist Eliminators 15
- Freeze Dryer Setup 16
- Vacuum Baffle Plate 17
- 8 Revision 004, 12/09 18
- Freeze-Drying Concepts 19
- Product Dependencies 20
- Sentry 2.0 Controls 21
- Button Functions 22
- LCD Display Functions 23
- User Options Menu 24
- Temperature Units 25
- Vacuum Units 25
- Relay Test 25
- Vacuum Pump Maintenance 25
- Alarms Menu 26
- Setpoints Menu 26
- Factory Options 27
- Interstage Control 28
- Calibration 28
- Vacuum Value 29
- 20 Revision 004, 12/09 30
- Basic Operation 31
- Quickseal Valves 32
- Operation Instructions 33
- Meltback 34
- Product Dryness End Point 35
- Stoppering (Optional) 35
- 26 Revision 004, 12/09 36
- Cold Trap Condenser 37
- Cold Trap Setup 38
- Optional Components 39
- Shelf Racks 40
- Liquid Nitrogen Trap 41
- Filter Trap 42
- BenchTop Cold Plate 43
- 34 Revision 004, 12/09 44
- General Maintenance 45
- Vacuum Tubing and Gaskets 46
- Condenser Gasket 46
- Refrigeration System 47
- Acrylic Parts 48
- Appendix A: Troubleshooting 49
- Product Melting 50
- Appendix 51
- 42 Revision 004, 12/09 52
- 44 Revision 004, 12/09 54
- Appendix D: Spare Parts List 55
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